Measurement of optical properties
Synthesis, cristallogenesis :
- microwave synthesis system CEM Discover ;
- cold chamber & glove box for atmosphere-controlled synthesis and/or storage ;
- Schlenk lines ;
- high volume synthesis reactors (5 to 10L) ;
- atmosphere and pressure controlled synthesis reactor (Büchi 500mL 6bars 200°C) ;
- evaporation and crystallization room ;
- lyophilizator, centrifuge, ball mill, ovens, columns, etc.
Caracterization & physicochemical analysis :
- X-ray diffraction – PANalytical X’Pert MPD with X’celerator (ambient temperature till 1000°C with HTK1200 Anton Paar chamber, atmosphere-controlled if needed) ;
- thermogravimetric & themodifferential analysis – Perkin Elmer Pyris Diamond & STA6000 with autosampler (40 samples) ;
- infrared spectrometer – Perkin Elmer Frontier FT-IR with MIR ATR module ;
- coupling of the Frontier with the STA6000 hrough transfer line Perkin Elmer TL8000 ;
- high temperature/high pressure chamber designed for the FT-IR measurements ;
- Inductively coupled plasma spectrometer – Perkin Elmer Avio 220 Max ;
- Scanning electron microscope with elemental analysis & cold device (-20,+50°C) – Hitachi TM1000, EDS Oxford Instuments, Peltier Deßen module ;
- evaluation of potential porosity through calculation – labmade method.
- spectrofluoromicroscope – Olympus IX51 ;
- spectrofluorimeter for solid/solution samples – Perkin Elmer LS55 ;
- spectrofluorimeter & quantum yield calculation for solid/solution samples – Horiba Jobin-Yvon Fluorolog III, integrating sphere F3018, photon sensors 200-850nm & 800-1600nm, control of the temperature (Horiba Peltier F3004, 263-383K & Oxford OptiStat CF & Oxford OptistatDry, 300-4K),
lifetime measurement (Horiba TCSCP FluoroHub – LED 20MHz 280, 300, 320, 340, 360nm & Horiba laser diodes 100MHz 375, 395, 405nm) ; - spectrofluorimeter & quantum yield calculation – Horiba Fluoromax, integrating sphere G8 (GMP SA)
- UV-visible spectrometer for solid/solution samples – Perkin Elmer Lambda 650 ;
- colorimeter – Majantys MSU 003 ;
- lumenmeter – Gigahertz-Optik X11 Optometer ;
- powermeter 254nm, 312nm, 365nm – Vilber Lourmat VLX-3.W ;
- powermeter PM100USB with S120VC photodiode 200-1100nm – Thorlabs
- stabilized & normalized calibration source D/Halogen – IDIL
- standard illumination chamber VeriVide (D50, D65, TL84, UV, A).
